Use of the Melles-Griot Reflectometer
Updated 29-Aug-02 E. Falco and M. Calkins
Unpack instrument with the exception of filters and spare light
bulbs. Determine the most convenient layout of instrument to
conduct measurements. Note - If measuring samples on a tabletop,
the power supply can be a source of vibrations which may adversely
affect measurements. Position power supply accordingly.
Attach test light source to power supply and power up. The test light
source is a 6 V, 20 W bulb. Do not exceed that voltage and power. It
takes a few minutes for the power supply to stabilize.
Use an RG58 coax cable to connect the light detector to the Melles
Griot Large Dynamic Range Amplifier (Input side). Note - The
amplifier can either be operated with internal batteries or with
external power transformer included in the case.
Measure direct (i.e., unreflected) light intensity. This can be
somewhat complicated depending on the location where the
measurements are taking place. Since the test light source is
essentially a traditional filament type bulb, the angle at which it
is mounted may cause the filament to sag, affecting output
intensity. Included with the reflectometer is an adjustable rig
mounted to a C-clamp. Secure the C-clamp to a solid surface and use
an allen wrench to rotate the rig to a position approximating as
close as possible the position where the measurements will take
place. Insert the light source at the end of the rig appropriate to
test conditions. Attach desired filter to end of light detector
making sure to align hash marks. Once the rig is secure you are
ready to measure the direct light intensity. Use the dial on the
Dynamic Range Amplifier to select appropiate range and read
measurement from LED.
Measure reflectivity of desired surface. Place the triangular plate
over surface to be measured. Insert test light source into orifice
on "base" side" of triangular plate. Insert desired filter into
other orifice and light detector into filter. Align the hash marks
between filter and detector. Select range on amplifier (should be
the same as unobstructed measurement). Take reading from LED. You
should adjust the height of the feet of the triangular plate until
the reading is maximized, otherwise your readings may be
spurious. Usually you only need adjust the foot at the tip of the
triangular plate to achieve happiness.
Repeat for all desired filters and surfaces.
Note: the Melles-Griot reflectometer that we used in 2001-2002 was
known to have suffered degradation (by August 2001) in its sensitivity
at wavelengths short of 500 nm. That explains the greater decline in
measured reflectivity than suggested by the trends in the plots. Bill Kindred
refurbished it, as of Jul 2003.